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An efficient synthesis of 2-[(5^/-(substituted phenyl)-1^/-phenyl) pyrazolyl] pyrroles III (a-m) starting from 2-acetyl pyrrole I and 2-[substituted benz-1/(propene-1//-one)] Pyrroles II (a-m), in the presence of phenyl hydrazine, 2-[(5^/-(4^//-substituted phenyl)-1^/-phenyl) pyrazolyl] pyrroles III (a-m) has been synthesized in microwave oven for the first time. On comparing with the classical methods, this method has advantages such as shorter reaction time, better yield, simple workup and environmental acceptability.